Our NMR instruments
N.D. Zelinsky Institute of Organic Chemistry,
Russian Academy of Sciences

Bruker WM 250

 Nuclei observed  1H, 13C,19F
 Probeheads  selective 1H 5mm
 selective 13C {1H} 5mm
 selective 13C {1H} 10mm
 selective 19F {1H} 5mm
 Temperature control  -100..+100 oC
 Workstation  Aspect 2000, 240K words memory,
 160 MB hard disk
 Software  Adakos 89 / DISN 94
 Installation year  1979 
 

WM 250 workplace
 Bruker WM 250 and Aspect 2000.

Useful pulse programs: COSYFAST, NOEFAST, ROESY, ROESYW, HOHAHA1d, HOHAHA1m

Used experiments: 1D and 2D experiments: homo- and heteronuclear correlations, NOESY, NOE difference, ROESY, selective 1H-1H decoupling

Added equipment: graphic display processor + color monitor; Hitachi hard disk (160 MB)

Self-made improvements:
  1. local network including Aspect and PC
  2. Faraday shields in all 5mm probeheads to enhance the line shape
  3. O1 and O2 connections for rotating frame experiments
  4. Computer-controlled relays for switching observer from 1H to X nucleus

WM-250 usage statistics


Bruker AM 300

 Nuclei observed  1H, 13C-15N, 31P-207Ag
 Probeheads  selective 1H 5mm
 BB {1H} 5mm
 BB {1H} 10mm
 inverse 1H {31P-207Ag}
 selective 15N{1H} 15mm
 triple 13C{1H, 14N} 10mm
 Temperature control  -100..+100 oC
 Workstation  Aspect 3000, 1M words memory,
 96 MB hard disk
 Software  Adakos 89 / DISB 94
 Installation year  1984 
 

AM 300 workplace
 Bruker AM 300 and Aspect 3000.
 
 
Useful pulse programs: HMQC, HMQCW, HMBC

Used experiments: all standard 1D and 2D experiments + inverse spectroscopy

Self-made improvements:
  1. local network including Aspect and PC
  2. Faraday shields in all 5mm probeheads to enhance the line shape
  3. O1 and O2 connections for rotating frame experiments
  4. BS-V 3DX used for 14N decoupling modernized for inverse spectroscopy

AM-300 usage statistics


Bruker DRX 500

 Nuclei observed  1H, 11B-207Ag
 Probeheads  BB {1H} 5mm
 triple inverse 1H {13C, 31P-207Ag}
  with Z-gradient coil
 Temperature control  -100..+100 oC
 Workstation  Slackware-10.2 Linux PC, 1GB memory,
 120GB hard disk
 Software  XwinNMR-3.6/TopSpin-1.3
 Installation year  1997 
 

DRX workplace
 Bruker DRX 500
electronics and PC workstation.

Used experiments: all standard 1D, 2D and 3D experiments with direct or inverse observation, 3D HMQC-TOCSY

DRX-500 usage statistics


Bruker AV 600

 Nuclei observed  1H, 11B-207Ag
 Probeheads  BB {1H} 5mm
 inverse 1H {13C, 31P-207Ag}
  with Z-gradient coil
 Temperature control  -100..+100 oC
 Workstation  PC RedHat Linux, 1GB memory,
 160GB hard disk
 Software  Liunx / Topspin-2.0 -2.1
 Installation year  2007 
 

DRX workplace
 Bruker AV 600

Used experiments: all standard 1D, 2D and 3D experiments with direct or inverse observation, 3D HMQC-TOCSY

AV-600 usage statistics


Bruker AC 200 (31)

 Nuclei observed  1H, 13C, 19F, 31P-207Ag
 Probeheads  selective 13C {1H} 5mm
 BB {1H} 10mm
 Temperature control  -100..+100 oC
 Workstation  Aspect 3000, 1M words memory,
 160 MB hard disk
 Software  Adakos 89 / DISR 94
 Installation year  1990 
 

AC workplace
 Aspect 3000 workstation

Useful pulse programs: SAB

Used experiments: standard 1D and 2D experiments: homo- and heteronuclear correlations, NOESY, NOE difference, ROESY, selective decoupling

Self-made improvements:
  1. local network including Aspect and PC
  2. Faraday shields in all 5mm probeheads to enhance the line shape

AC-200 (31) usage statistics


Bruker AC 200 (33)

 Nuclei observed  1H, 13C, 19F, 31P-207Ag
 Probeheads  selective 13C {1H} 5mm
 selective 19F {1H} 5mm
 BB {1H} 10mm
 CP/MAS 15N-31P {1H} 8mm
 Temperature control  -100..+100 oC
 Workstation  Aspect 3000, 1M words memory,
 160 MB hard disk, CP/MAS cabinet
 Software  Adakos 89 / DISR 94
 Installation year  1988 
 

Useful pulse programs:
SAB

Used experiments: standard 1D and 2D experiments: homo- and heteronuclear correlations, NOESY, NOE difference, ROESY, selective decoupling

Self-made improvements:
  1. local network including Aspect and PC
  2. Faraday shields in all 5mm probeheads to enhance the line shape

AC-200 (33) usage statistics


NMR Center Statistic page

Helium level and drift of field and X,Y,Z shimms

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